Evaluation of a high-resolution micro-sized magic angle spinning (HR[small mu ]MAS) probe for NMR-based metabolomic studies of nanoliter samples - CEA - Commissariat à l’énergie atomique et aux énergies alternatives Access content directly
Journal Articles Analytical Methods Year : 2016

Evaluation of a high-resolution micro-sized magic angle spinning (HR[small mu ]MAS) probe for NMR-based metabolomic studies of nanoliter samples

Abstract

This study evaluates the performances of a recently introduced 1 mm HR[small mu ]MAS NMR probe for metabolic profiling of nanoliter samples. It examines essential NMR criteria such as spectral data qualities and repeatability, and experimental practicality. The report also discusses the difficulties related to the sample preparation in HR[small mu ]MAS experiments and considers possible solutions and improvements.
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Dates and versions

cea-01380672 , version 1 (13-10-2016)

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Tuan Nghia Duong, Yuki Endo, Takahiro Nemoto, Hiroshi Kato, Anne-Karine Bouzier-Sore, et al.. Evaluation of a high-resolution micro-sized magic angle spinning (HR[small mu ]MAS) probe for NMR-based metabolomic studies of nanoliter samples. Analytical Methods, 2016, 8, pp.6815-6820. ⟨10.1039/C6AY01654E⟩. ⟨cea-01380672⟩
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